电工钢 ›› 2025, Vol. 7 ›› Issue (5): 25-.

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常化与退火温度对薄规格高硅无取向硅钢组织、织构演变及磁性能的影响

黄晓磊,王银平,刘海涛   

  1. 东北大学 数字钢铁全国重点实验室,辽宁 沈阳 110819
  • 出版日期:2025-10-28 发布日期:2025-10-21

Effect of normalization and annealing temperatures on the microstructure, texture evolution and magnetic properties of thin⁃gauge high⁃Si non⁃oriented silicon steels

HUANG Xiaolei,WANG Yinping,LIU Haitao   

  1. State Key Laboratory of Digital Steel,Northeastern University, Shenyang 110819, China
  • Online:2025-10-28 Published:2025-10-21

摘要: 以3.4 %Si无取向硅钢为研究对象,系统研究了常化温度和退火温度对微观组织、织构特征以及0.25 mm厚度成品板磁性能的综合影响规律。结果表明:通过不同温度的常化处理,可以使热轧板组织实现再结晶及晶粒长大,并影响成品板的再结晶组织、织构及磁性能。随着常化温度的升高,晶粒尺寸明显增大,组织均匀性得到改善,最终退火板中λ纤维再结晶织构(<001>∥ND)明显增强,γ纤维再结晶织构(<111>∥ND)减弱,并且晶粒尺寸增大。所以,随着常化温度的升高,磁感应强度B50逐渐增高,低频铁损P1.5/50逐渐降低,但高频铁损P1.0/400先降低后升高。通过不同温度的退火处理也可以改变再结晶组织、织构及磁性能。随着退火温度的升高,退火板中晶粒尺寸明显增大,λ纤维再结晶织构逐渐减弱,γ纤维再结晶织构逐渐增强。所以,随着退火温度的升高,磁感应强度B50先略增高后逐渐降低,低频铁损P1.5/50逐渐降低,但高频铁损P1.0/400先降低然后逐渐升高。在常化温度为910 ℃、退火温度为900 ℃时,可获得较高的磁感应强度和较低的铁损指标组合:磁感应强度B50为1.70 T,低频铁损P1.5/50为2.29 W/kg,高频铁损P1.0/400为13.27 W/kg。

关键词: 无取向硅钢, 常化温度, 退火温度, 组织, 织构, 磁性能

Abstract: This study focused on a 3.4 %Si non⁃oriented silicon steel. The comprehensive effects of normalization temperature and annealing temperature on the microstructure, texture characteristics, and magnetic properties of the 0.25 mm⁃thick products were studied systematically. The results indicated that normalization treatment at different temperatures could achieve recrystallization and grain growth in the hot⁃rolled sheet, thereby influencing the recrystallized microstructure, texture, and magnetic properties of the final products. With increasing the normalization temperatures, the average grain sizes of the normalized sheets increased obviously, and the microstructure uniformity was improved. In the final annealed sheets, the λ⁃fiber recrystallization texture (<001>∥ND) was notably strengthened, while the γ⁃fiber recrystallization texture (<111>∥ND) was weakened, accompanied by increased grain size. Therefore, with increasing the normalizing temperature, the magnetic induction B50 gradually raised, the low⁃frequency iron loss P1.5/50 gradually decreased, while the high⁃frequency iron loss P1.0/400 first decreased and then increased. In addition, annealing treatment at different temperatures had an important influence on the recrystallization microstructure, texture, and magnetic properties. As the annealing temperature increased, the grain sizes of the final annealed sheets significantly increased, and the λ⁃fiber recrystallization texture was weakened gradually, but the γ⁃fiber recrystallization texture was strengthened progressively. Thus, with increasing the annealing temperature, the magnetic induction B50 initially showed a slight increase followed by a gradual decrease, and the low⁃frequency iron loss P1.5/50 progressively declined, while the high⁃frequency iron loss P1.0/400 first decreased and then gradually raised. An optimal combination of high magnetic induction and low iron loss was obtained at a normalization temperature of 910 ℃ and annealing temperature of 900 ℃, with the following magnetic properties: magnetic induction B50 of 1.70 T, low⁃frequency iron loss P1.5/50 of 2.29 W/kg, and high⁃frequency iron loss P1.0/400 of 13.27 W/kg.

Key words: non?oriented silicon steel, normalization temperature, annealing temperature, microstructure, texture, magnetic properties