电工钢 ›› 2025, Vol. 7 ›› Issue (5): 1-.

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Fe⁃3 %Si平面流铸超薄带退火组织织构与磁性能演变研究#br#

张 宁,涂 杨,傅 超,孟 利   

  1. 钢铁研究总院有限公司 冶金工艺研究所,北京 100081
  • 出版日期:2025-10-28 发布日期:2025-10-21

Study on the annealing microstructure, texture and magnetic properties evolution of Fe⁃3 % Si ribbons prepared by planar flow casting#br#

ZHANG Ning, TU Yang, FU Chao, MENG Li   

  1. Metallurgical Technology Institute, Central Iron and Steel Research Institute Co., Ltd., Beijing 100081, China
  • Online:2025-10-28 Published:2025-10-21

摘要: 采用平面流铸技术可制备Fe⁃3 %Si硅钢超薄带,本文研究厚度~0.05 mm的平面流铸超薄带在退火过程中的组织织构与磁性能演变。结果表明,平面流铸带贴辊面与自由面均观察到超细晶组织,织构主要表现为{001}(<001>//ND)织构与铜型({112}<111>)织构。退火过程中,退火温度对组织演变存在显著影响:950 ℃退火时,超薄带自由面及贴辊面晶粒均长大程度有限;当退火温度增加至1 050 ℃时,部分晶粒表现出强长大优势,但保温3 h后仍有大量细小晶粒存在。总的来说,退火前后织构类型未发生转变,{001}织构有所增强体现了此类晶粒的长大优势。磁性能方面,退火前后超薄带的磁感应强度B5000几乎维持在1.68 T左右;950 ℃退火时退火时间延长,并未带来铁损P1.0/400的显著变化,而1 050 ℃退火时因组织粗化,使得铁损值随保温时间的延长从>40 W/kg逐渐降至~20 W/kg。

关键词: 平面流铸, Fe?3 %Si, 退火, 组织, 织构, 磁性能

Abstract: Planar flow casting technique can be used to prepare Fe⁃3 %Si ribbons. This study investigated the annealing microstructure, texture, and magnetic properties evolution of Fe⁃3 %Si ribbons with a thickness of ~0.05 mm prepared by planar flow casting. The results show that ultra⁃fine microstructures are observed on both the wheel surface and free surface of the planar flow casting ribbons, with the texture primarily characterized by {001}(<001>//ND) and copper ({112}<111>) texture. During annealing, annealing temperature significantly influences the microstructure evolution. That is, when annealed at 950 ℃, grain growth on both surfaces of the Fe⁃3 %Si ribbons is limited; when the annealing temperature increases to 1 050 ℃, some grains exhibit strong growth advantages, while a number of fine grains still remain after being annealed for 3 hours. Overall, the type of main texture components does not change along annealing, and the enhancement of {001} texture implies the growth advantage of {001} grains. In terms of magnetic properties, the magnetic induction B5000 remains~1.68 T before and after annealing. When annealed at 950 ℃, prolonging annealing time does not lead to significant changes in the iron loss P1.0/400, whereas at 1 050 ℃, the iron loss gradually decreases from >40 W/kg to ~20 W/kg due to the microstructural coarsening with the extended holding time.

Key words: planar flow casting, Fe?3 %Si, annealing, microstructure, texture, magnetic properties