电工钢 ›› 2023, Vol. 5 ›› Issue (3): 1-7.

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变形温度对含铜取向硅钢热变形过程抑制剂析出的影响研究

马胜梅1,3,金自力2,3   

  1. 1.包头职业技术学院 材料工程系, 内蒙古 包头 014030;
    2.内蒙古科技大学 材料与冶金学院, 内蒙古 包头 014010;
    3.内蒙古自治区 新金属材料重点实验室, 内蒙古 包头 014010
  • 出版日期:2023-06-28 发布日期:2023-06-26

Effect of deformation temperature on the inhibitor precipitation of Copper-containing grain-oriented silicon steel during hot deformation

MA Shengmei1,3, JIN Zili2,3   

  1. 1.Department of Materials Engineering, Baotou Vocational and Technical College, Baotou 014010, China;
    2.School of Material and Metallurgy,Inner Mongolia University of Science and Technology, Baotou 014010,China;
    3.Inner Mongolia Key Laboratory of New Metal Materials, Baotou 014010, China
  • Online:2023-06-28 Published:2023-06-26

摘要: 对实验取向硅钢分别在1 100 ℃和970 ℃温度以30 %压下量轧制,热轧后分别在轧制温度下保温,利用热场发射扫描电子显微镜,观察变形温度和保温时间对抑制剂粒子析出的尺寸分布和体积分数的影响,通过电感耦合等离子体质谱仪分别对不同工艺下取向硅钢轧制表面、近表面和中心处Cu和Mn的析出量进行测定。结果表明:热轧过程中大尺寸粒子是Cu和Mn的复合析出物,热轧温度和随后保温时间对含锰抑制剂的析出没有明显影响,热轧温度越低(970 ℃),含铜抑制剂的析出越快,但保温时间对含铜抑制剂的进一步析出影响不大,仍保持在变形后的析出状态。并在高温(1 100 ℃)热轧后的保温过程可以增大含铜抑制剂的析出量。

关键词: 变形温度, 取向硅钢, 抑制剂, 析出

Abstract: The tested grainoriented silicon steel was deformed at 30 % rolling reduction at 1 100 ℃ and 970 ℃ respectively, and was kept warm at rolling temperature. The influences of the rolling temperature and the holding time on the size distribution and volume fraction of inhibitor particles were observed by thermal field emission scanning electron microscopy. The precipitation amounts of Cu and Mn at the rolling surface,near surface and center of the grainoriented silicon steel under different processes were determined by inductively coupled plasma mass spectrometer. The results showed that the large size particles are the composite precipitates of CuS and MnS during the hot rolling process. The hot rolling temperature and holding time have no obvious impact on the precipitation of Mn-containing inhibitors. The lower the hot rolling temperature (970 ℃), the faster the precipitation of Copper-containing inhibitors is, but the holding time has no impact on the further precipitation of Copper-containing inhibitors, and inhibitors still remains in the precipitation state after deformation. With the extension of the holding time, the precipitation amount of copper-containing inhibitors increases after high temperature(1 100 ℃) thermal deformation/hot rolling.

Key words: deformation temperature, grain-oriented silicon steel, inhibitor, precipitation