取向高硅钢的制备与表征

电工钢 ›› 2019, Vol. 1 ›› Issue (1): 8-10.

取向高硅钢的制备与表征

刘刚，唐柏金，刘新丽，雷明，郑晓峰

东北大学材料科学与工程学院，辽宁沈阳 110819

出版日期:2019-10-28 发布日期:2020-07-13

Preparation and characterization of oriented high silicon steel

LIU Gang, TANG Baijin, LIU Xinli, LEI ming, ZHEN Xiaofeng

College of Material Science and Engineering, Northeastern University, Shengyang 110819，China

Online:2019-10-28 Published:2020-07-13

摘要/Abstract

摘要： 采用粉末包埋法对成品Si的质量分数3 %的取向硅钢进行固体渗硅和扩散退火，并对样品的组织、物相、织构和磁性能进行测试分析。结果表明：在800 ℃、硅粉+（质量分数0.5 %）卤化物+填充剂的条件下，在较短的时间（10 min）内即可在Si的质量分数3 %的取向硅钢上制备出表面平整、内部致密、与基体结合良好的渗硅层；经过扩散退火后，Goss织构能够完全保留下来，同时高频铁损显著降低（37 %~63 %）。证明固体渗硅技术可以制备出磁性能优异的取向高硅钢。

关键词: 取向高硅钢, 固体渗硅, 扩散退火, 制备

Abstract: The structure, phase, texture and magnetic properties of the samples of the finished grain oriented silicon steel with Si content of 3% were tested and analyzed after solid siliconizing and diffusion annealing by pack cementation. The results showed that: the silicon permeable layer with smooth surface, dense interior and good bonding with matrix can be prepared on the oriented silicon steel with Si content of 3 % in a short time (10 min) under the condition of 800 ℃ and silicon powder + (mass fraction 0.5 %) halide + filler, and Goss texture can be completely retained with high frequency iron loss reduced significantly (37 %~63 %) after diffusion annealing. It has been proved that solid silicon osmosis technology can prepare oriented high silicon steel with excellent magnetic properties.

Key words: grain oriented high silicon steel, solid siliconizing, diffusion annealing, preparation

刘刚, 唐柏金, 刘新丽, 雷明, 郑晓峰. 取向高硅钢的制备与表征[J]. 电工钢, 2019, 1(1): 8-10.

LIU Gang, TANG Baijin, LIU Xinli, LEI ming, ZHEN Xiaofeng. Preparation and characterization of oriented high silicon steel[J]. Electrical Steel, 2019, 1(1): 8-10.