电工钢 ›› 2022, Vol. 4 ›› Issue (1): 18-.

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钇元素对6.5 % Si无取向硅钢组织、高温拉伸及断裂机制的影响

李昊泽1,李民1,2,刘德壮3,李奥迪1,马颖澈1   

  1. 1.中国科学院金属研究所 师昌绪创新中心,辽宁 沈阳 110016;2.沈阳航空航天大学 材料科学与工程学院,辽宁 沈阳 110136;3.沈阳工业大学 材料科学与工程学院,辽宁 沈阳 110870
  • 出版日期:2022-02-28 发布日期:2022-02-21

Effects of yttrium on microstructure, elevatedtemperature tensile properties and fracture mechanism of 6.5 % Si non-oriented electrical steel#br#

LI Haoze1,LI Min1,2,LIU Dezhuang3,LI Aodi1,MA Yingche1   

  1. 1.Shi changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China;2.College of Materials Science and Engineering, Shenyang Areospace University,Shenyang 110136, China;3.School of Materials Science and Engineering, Shenyang University of Technology, Shenyang 110870, China
  • Online:2022-02-28 Published:2022-02-21

摘要: 通过微观组织表征、高温拉伸和断口形貌分析,研究了钇(Y)元素对 6.5 % Si无取向硅钢组织、高温拉伸及断裂机制的影响。研究结果表明,添加Y元素可以在钢液中形成YS和YP的复合析出。YS和YP可以充当异质形核基底,提高形核率,细化凝固组织。热轧组织不均匀,由表层至芯部分别形成等轴晶、等轴晶/拉长晶和拉长晶的混合组织。退火后,热轧变形组织转变为等轴晶,含Y实验钢的退火组织得到明显细化。500 ℃时效处理后,含Y实验钢具备较低的有序度,300 ℃的拉伸断口呈现韧性断裂特征,断后伸长率达到20.2 %。相反,无Y实验钢发生脆性断裂,断后伸长率仅为2.1 %。研究结果证实,Y元素可以通过组织细化和降低有序度提高6.5 % Si无取向硅钢的中温塑性。

关键词: 6.5 % Si无取向硅钢, 稀土, 微观组织, 有序度, 拉伸

Abstract: The effects of yttrium(Y) on microstructure, elevatedtemperature tensile properties and fracture mechanism of 6.5 %  Si non-oriented electrical steel were investigated by means of microstructure characterization, high-temperature tensile test and fracture analysis. The results showed that the doping of Y introduced composite Y rich precipitates (YS/YP) in the melt. YS and YP precipitates were qualified for heterogeneous nucleation agents, which thus raised the nucleation rate and refined the solidification microstructure. The hot rolling microstructures were inhomogeneous through the thickness. Three distinct layers characterized by equiaxed grains, a mixture of equiaxed and elongated grains and completely elongated grains were detected at the surface, subsurface and center layers, respectively. After annealing, the hot rolling microstructures were transformed into equiaxed structures. The annealing microstructure of the experimental steel doped with Y was significantly refined. After aging at  500 ℃, the experimental steel doped with Y showed a lower ordering degree and a ductile fracture morphology at  300 ℃. The tensile ductility approached as high as 20.2 %. On the contrast, the experimental steel undoped with Y fractured brittlely and the tensile ductility was only 2.1 %. The results verified that the doping of Y in 6.5 % Si non-oriented electrical steel could improve the intermediate temperature ductility by refining the microstructure and lowering the ordering degree. 

Key words: 6.5 % Si non-oriented electrical steel, rare earth, microstructure, ordering degree, tensile test