炼钢 ›› 2022, Vol. 38 ›› Issue (6): 6-13.

• 凝固与浇铸 • 上一篇    下一篇

镁处理对AISI4130钢组织及夹杂物的影响

刘  颖,刘建华,何  杨,谢仲豪   

  1. 北京科技大学 工程技术研究院,北京 100083
  • 出版日期:2022-12-05 发布日期:2022-12-02

Effect of Mg addition on solidification structure and inclusions in AISI4130 steel

  • Online:2022-12-05 Published:2022-12-02

摘要: 提高铸坯等轴晶比例、细化组织对提高钢的力学性能具有重要意义。对AISI4130钢进行镁处理试验,采用SEM、低倍组织观察及微观组织分析,分析镁对钢中夹杂物控制、凝固组织及微观组织影响的内在机理。研究表明镁处理后铸锭等轴晶比例增加,平均晶粒尺寸减小;当镁质量分数在0.002 %~0.006 %时,等轴晶比例随镁含量增加而增加;镁处理后钢中Al2O3、MnS变质为Al-O-Mg-Mn-S复合夹杂物,镁含量较高时MgS-MnS成为钢中最主要夹杂物;镁处理后钢中1~2 μm的夹杂数量密度明显增加,5 μm以上的夹杂物占比显著降低;镁处理试样组织中有明显以镁氧化物复合夹杂粒子为核心长大的针状铁素体,镁质量分数为0.009 %和0.023 % 的AISI4130铸锭显微组织为相互交错的细小针状铁素体组织,冲击韧性显著提升,冲击功平均值约为镁处理前AISI4130钢的3倍。

关键词: 镁处理, 凝固组织, 夹杂物, 针状铁素体, 异质形核

Abstract: Increasing the proportion of equiaxed grains and refining the microstructure are of great significance to improve the mechanical properties of steel. In this study, AISI4130 steel was treated with magnesium. SEM, macrostructure observation and microstructure analysis were used to analyze the internal mechanism of the influence of Mg on inclusions control, solidification structure and microstructure of steel. The results show that the proportion of equiaxed grains increases and the average grain size decreases after Mgtreatment. When the Mg mass fraction is between 0.002 %–0.006 %, the proportion of equiaxed crystal increases with the increase of magnesium content.After Mg-treatment, the Al2O3, MnS had changed to Al-O-Mg-Mn-S,When the content of Mg is high, the MgS-MnS becomes the most important inclusion in the steel. In the Mg-treatment steel, the density of inclusions of 1-2 μm increased significantly, and the proportion of inclusions of more than 5 μm decreased. The steel after Mg-treatment has acicular ferrite at Mg-O inclusions grow core. The microstructure of AISI4130 ingots with Mg mass fraction of 0.009 % and 0.023 % is staggered fine acicular ferrite, and its impact toughness are significantly improved, and the average impact energy is about three times that of non-Mg-treatment.


Key words: Mg-treatment, solidification structure, inclusion, acicular ferrite, heterogeneous nucleation