Electrical Steel ›› 2019, Vol. 1 ›› Issue (1): 23-28.
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SHEN Minghui,YANG Jiaxin,GUO Xiaolong,LUO Xingen, GAO Yang, CHENG Xiangwei
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Abstract: The annealing processes of low temperature grainoriented silicon steel which containing bismuth(Bi)and Bifree components have been studied by interrupting test,and the magnetic properties were measured by magnetic determinator (MPG200D), the evolution of texture and grain size was analyzed by Xray diffraction (XRD) and optical microscopy. The results showed that the primary grain size decreased and the secondary recrystallized grain size increased to 20~60 mm after the addition of Bi element. The onset temperature of secondary recrystallization was increased significantly after the addition of Bi element,and the temperature ranges of grain abnormal growth on containing Bi and Bifree sample were 1 080~1 100 ℃ and 1 060~1 080 ℃ respectively. The texture analysis showed that as the high temperature annealing temperature increased, the {111} and {100} textures were gradually weakened, the {110} texture and Goss texture were gradually enhanced. The texture transformation temperatures of containing Bi and Bifree samples were 1 100 ℃ and 1 080 ℃ respectively, then the Goss texture density and volume fraction increased gradually. The Goss texture density and volume fraction of Bicontaining samples were higher than those of Bifree samples.
Key words: low temperature grainoriented silicon steel, high temperature annealing, texture, bismuth(Bi), grain size
SHEN Minghui, YANG Jiaxin, GUO Xiaolong, LUO Xingen, GAO Yang, CHENG Xiangwei. Effect of Bi on microstructure and texture during high temperature annealing of low temperature grainoriented silicon steel[J]. Electrical Steel, 2019, 1(1): 23-28.
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http://www.bwjournal.com/dgg/EN/Y2019/V1/I1/23